MTBSTFA
MTBSTFA is a Silylation Reagent for GC Derivatization that replaces active hydrogens to form
t-BDMS derivatives. Derivatization is usually complete upon dissolution with this exceptionally strong, yet mild silylating reagent. MTBSTFA derivatives are 104 times more stable to hydrolysis than their corresponding TMS derivatives and produces easily interpreted mass spectra for GC/MS.
Addition of
t-BDMCS catalyzes reactions of hindered alcohols and amines.
Physical and Chemical Properties
Suggested Storage Conditions: Cool Place
Use: Silylation Reagent for GC
Appearance: Clear, colorless liquid
BP: 343ºF (172ºC)
MF: C
9H
18F
3NOSi or (C
9H
18F
3NOSi + C
6H
15ClSi)
FW: 241.33 g/mol (MTBSTFA) or {241.33 g/mol (MTBSTFA) + 150.72 g/mol (
t-BDMCS)}
Specific Gravity (H
20 = 1.0): 1.023
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MTBSTFA; MTBSTFA + 1% t-BDMCS; N-Methyl-N-(t-butyldimethylsilyl) trifluoroacetamide
CAS [77377-52-7 MTBSTFA; 18162-48-6 t-BDMCS]
| Product | Size | Regis Product # | U.S. Price |
|
| MTBSTFA | 5 x 1 gram | 270241 | $91.08 |  |
| MTBSTFA | 2 x 5 gram | 270242 | $93.15 |  |
| MTBSTFA | 25 gram | 270243 | $170.78 |  |
| MTBSTFA + 1% t-BDMCS | 5 x 1 gram | 270141 | $81.00 |  |
| MTBSTFA + 1% t-BDMCS | 2 x 5 gram | 270142 | $91.08 |  |
| MTBSTFA + 1% t-BDMCS | 25 gram | 270143 | $170.78 |  |
| MTBSTFA + 1% t-BDMCS | 10 x 1 gram | 270144 | $139.73 |  |